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1996, Physica C: Superconductivity
We have investigated the hysteresis in the AC susceptibility of granular YBCO superconductors when the DC field is cycled. A crossover point is observed where the susceptibility X' in decreasing fields becomes more diamagnetic than for increasing fields, and this is investigated as a function of temperature, AC field amplitude and frequency. The behavior is consistent with the variation of the AC penetration depth with these variables and with a reduced flux density of the intergrain regions on field reversal. The zero field cooled behavior of the second harmonic X2 as well as the behavior of X' in field cooled conditions, are also reported. The DC field dependence of X' is analyzed using the low amplitude, linear response region approximations.
Physica C: Superconductivity, 1994
The AC susceptibility, x~,-( T), with superimposed DC magnetic field, H F", has been measured as a function of temperature in bulk sintered LaSrCuO, for zero-field cooled (ZFC) and field-cooled (FC) samples. Results are analyzed within Rim's critical-state model extended to a granular superconductor, where the role of grains is to determine the temperature-dependent effective permeability, &u(T), and the effective intergranular local field, H,*( H, Dc, T), which depends on the applied field, H,"c and the thermal and magnetic history, accounting for the observed hysteresis. A method to determine field-independent intergranular critical-state parameters (critical current at zero field and temperature-dependent density of pinning forces as well as h( T) ) and the proper scaling of H,@( H F, T) for ZFC and FC conditions is described. The calculated AC susceptibility for the whole temperature range for both magnetic conditions reproduces the main features of the experimental results. 0921-4534/94/$07.00 0 1994 Elsevier Science B.V. All rights reserved SSDIO921-4534(94)02309-3
Bulletin of Materials Science, 1994
Experimental data on the real (Z') and imaginary (g') parts of AC magnetic susceptibility as a function of DC bias field (/4) shows the effect of trapped flux in granular high T c superconductors. The aim was to substantiate our recent theoretical findings on the basis of a two-component critical state model suitable for granular high T c superconductors. Stress has been given to understanding the origin of hysteresis in Z'(H) and Z*(/-/). It was seen in the experimental data that above a certain value of DC field range irreversibility appears in z'(H) and Z*(/-/) creating hysteresis like loops. Comparison of data with calculated loops shows good agreement. Z'(H) and z'(H) curves show considerable asymmetry in pre~nce of trapped flux.
Physica C: Superconductivity, 1991
We have measured the longitudinal ac electrical field in polycrystalline YtBazCu307.~ compounds (~ 0. I) associated with low frequency ac electrical currents (v s 16 KHz, je s 1.5 A/cm ~) in the presence of an external dc magnetic field up to 0.5 T. To within the resolution of our measurements {0.5 ~V/cm} no frequency-dependent effects were o~served in the temperature range of room temperature down to 77 K.
Physica C: Superconductivity, 2002
A phenomenological theory to describe the electromagnetic properties of granular superconductors, based on known bulk superconductors expressions and conventional Josephson's junctions tunneling currents, is presented and successfully used to fit distinct experimental results for the magnetic susceptibility χ as a function of the temperature and the applied magnetic field of rather different samples.
Cryogenics, 1993
The experimental hysteretic behaviour of the transport critical current density Jc(He) observed in granular YBa2Cu307_ ~ has been compared with the analogous theoretical curves resulting from a well known model based on the effect of flux trapped by the superconducting grains at the intergranular junctions. The magnetization of the grains was calculated for different values of maximum applied field Hm using the Bean model; at the same time the statistical distribution of the qualities of the junctions was taken into account. This approach was seen to predict the evolution of hysteretic Jc(He) curves for different values of Hm with reasonable accuracy.
2014
We report on magnetization and magnetoresistance measurements of polycrystalline Y3Ba5Cu8O18 superconductor (Y358), prepared by solid state reaction in order to study the correlation between the magnetic irreversibility line and the zero electric resistance as a function of applied field. The magnetization measurements were performed using a MPMS-XL SQUID magnetometer and the magnetoresistance measurements were made using a PPMS, both from Quantum Design, up to 1 T. The granular microstructure was confirmed by scanning electron microscopy. In this case the grain junctions are weaker than in the Y123 system and the effect of the applied field on the grain couplings is much stronger. Consequently, in our sample the zero resistance line shifts away from the irreversibility line and is lower by more than 15 K at 1 T. We explain our results in terms of the superconducting glass model and in comparison with results obtained in other materials from the YBaCuO family.
Physica C: Superconductivity, 2001
The hysteretic behavior of the superconducting critical current density J c (B a ) dependence under low applied magnetic ®elds B a < 50 mT of polycrystalline Bi 1:64 Pb 0:36 Sr 2 Ca 2 Cu 3 O y samples was investigated. All the samples were prepared from the same powder but subjected to dierent pressures ranging from 40 to 250 MPa before the last heat treatment. The samples were characterized by scanning electron microscopy and X-ray powder diraction analysis. The magnetic behavior of the superconducting grains was studied by measuring magnetization versus applied magnetic ®eld in powder samples. The J c (B a ) data are discussed within the scenario of the three-level superconducting system. Ó 2001 Published by Elsevier Science B.V.
Solid State Communications, 1988
Alkali (Ak) ion (i.e., Ak = Li, Na, K, Cs) substitution for Ba has been made in granular Y~Ba2Cu307_ ~, superconducting ceramics. The synthesis temperature is lowered to 800°C. The electrical resistivity R and the magneto-resistivity have been measured as a function of temperature T. For the Li substituted sample, a marked change in the critical temperature T¢ is observed. It is explained by a modification of the local density of states due to Li substitution (or insertion) in Cu-O planes. In this respect, BCS-like expressions for discussing Tc are useful. In the other samples, R(T) curves show two critical temperatures, interpreted as arising from the coexistence of two superconducting phases: one contains the substitution element, the other contains the original (1-2-3) phase. The Li sample presents some anomalous hysteresis at low field.
IEEE Transactions on Applied Superconductivity, 2008
In this paper, the crossed field demagnetization effect of the bulk type-II superconducting materials in a variety of external magnetic field condition has been investigated both numerically and experimentally. A melt-textured YBCO bulk sample was magnetized along the axial direction and after that a transverse field perpendicular to the central axis applied. The collapse of the original trapped field was measured using a Quantum Design Physical Property Measurement System. A numerical solver based on critical state model is proposed to simulate the measured results.
Physics Letters A, 1992
Low field magnetization curves of cylindncal samples ofhigh-T. granular superconductors are calculated analytically by means ofa critical state model based on a Josephson junction array description ofthis class of superconductors.
Physica C-superconductivity and Its Applications, 1999
A comparative study of the hysteretical behavior of the zero resistance critical temperature for YBa Cu O , 2 3 7 yd Ž. Ž. BiPb Sr Ca Cu O and HgRe Ba Ca Cu O superconducting ceramics was performed at low magnetic fields 2 2 2 3 10qd 2 2 3 8qd Ž. under 400 Oe. The results were compared with those obtained through the magnetic hysteresis of the critical current density, showing good agreement in most cases. The qualitative explanation of the observed hysteresis in terms of intragranular flux trapping of the superconducting grains satisfies YBaCuO and BiSrCaCuO materials, but modifications might be necessary in the case of HgBaCaCuO.
Physica C: Superconductivity, 2000
Ž. Ž. The hysteresis of the transport critical current of YBa Cu O Hg,Re Ba Ca Cu O and BiPb Sr Ca Cu O 2 3 7 yd 2 2 2 8qd 2 2 2 3 10qd polycrystals was studied. While the first two systems display qualitatively similar hysteretical patterns, the third one behaves differently. The experimental results are interpreted in terms of a phenomenological model which considers the effects of the magnetization in the grains on the intergranular weak links as responsible for the observed hysteresis. The hysteresis of the transport critical current is discussed on the light of the microstructural features of the samples, concluding that the shape and disposition of the grains do not account in a straightforward fashion for the differences in the hysteretical behavior.
Journal of Superconductivity and Novel Magnetism, 2013
The magnetovoltage measurements (V-H curves) with different sweeping rates (dH/dt) of the external magnetic field in Ag-added polycrystalline YBa 2 Cu 3 O 7−x sample (YBCO/Ag) were investigated. The measurements of V -H curves were carried out as functions of the transport current (I ) and temperature (T ). Upon cycling H , all V -H curves measured for different values of I exhibit a clockwise hysteresis effects in forward region. The hysteresis effects in the V -H curve were interpreted in terms of two-level magnetic system, which considers the superposition of the external magnetic field and the local magnetic fields in the intergrain boundaries induced by magnetic dipole moment of neighbor superconducting grains. The analysis of magnetovoltage data showed that the flux trapping in the junction network has a negligible effect on the evolution of the V -H curves and the irreversibilities arise mainly from the flux trapping inside the grains. It is shown that the width of V -H curves shows a universal scaling behavior with respect to the applied current below the critical temperature T c . The comparison of V -H curves of the YBCO/Ag sample with those of YBCO shows that adding Ag to the superconducting structure weakens the pinning properties of Josephson medium and provokes the instabilities in measured dissipation. The presence of Ag in the superconducting matrix causes marked decrease in hysteresis effects and makes the V -H curves dH/dt dependent. At high values of dH/dt, the instabilities and plateau regions in V -H curves increase significantly as compared to those of observed in YBCO. In addition, the interrelation between the evolution of V -H curves obtained for different values of I and the critical current I c was demonstrated experimentally.
Physical Review B, 2008
We report on magnetization and magnetoresistance measurements of single-crystal, melt-processed, and polycrystalline YBa 2 Cu 3 O 7−␦ samples with the purpose of disclosing the connection between the magnetic irreversibility limit and the zero resistance temperature point as a function of applied field in the above samples with very different superconducting granularities. Another goal is to find out how much the applied fields degrade the grain couplings and the electric conductivity for the different field-current configurations. In homogeneous superconductors, the magnetic irreversibility line is well known as a limit below which an electric current different from zero can flow without resistance. Our data for the single crystal with a weak superconducting granularity closely follow this rule. However, the results on the other samples are quite different. Normally, good-quality melt-processed YBa 2 Cu 3 O 7−␦ samples do not exhibit the signature of superconducting granularity. Nevertheless, x-ray analysis of our melt-processed sample, containing 30 wt % of the Y 2 BaCuO 5 phase, shows considerable misalignment of the crystallite c axis, which weakens the grain couplings and hence is expected to result in superconducting granularity. Effectively, the magnetic irreversibility lines for H ʈ c axis as well as for H ʈ ab plane exhibit, in the low-field region, the usual signature of superconducting granularity. On the other hand, the zero resistance data for increasing fields along the c axis and J ʈ ab plane split away from the irreversibility line toward the lower-temperature side. Nevertheless, for H ʈ J ʈ ab plane, the zero resistance data closely follow the irreversibility line up to the highest applied fields. In the polycrystalline YBa 2 Cu 3 O 7−␦ sample, in which the grain junctions are much weaker, the effect of an increasing applied field on the grain couplings is much stronger. The zero resistance line is already split from the irreversibility line and is lower by more than 17 K at 8 kOe. Our present measurements provide good quantitative data for the discrepancy between the zero resistance and magnetic irreversibility lines. We explain these features in terms of the superconducting glass model.
Physica C: …, 1998
The low-field magnetic response of a physical system consisting of eight superconducting spherical grains in a cubic arrangement is studied by means of a three-dimensional Josephson junction network. The lower threshold field for this ™ system is numerically studied as a function of the inclination of the externally applied magnetic field H with respect to the z-axis. q 1998 Published by Elsevier Science B.V. All rights reserved. PACS: 74.80.B; 74.25.Ha; 74.50.q r
Europhysics Letters (EPL), 1996
PACS. 74.60Ge -Flux pinning, flux creep, and flux-line lattice dynamics. PACS. 74.72Bk -Y-based compounds. PACS. 74.80Bj -Granular, melt-textured, and amorphous superconductors; powders.
Physica C: Superconductivity, 1992
Results from AC susceptibility x(H, T) and resistivity p(H, T) measurements on YBa2Cu307 single crystals, in the mixed state by applying magnetic fields H parallel to the c-axis, strongly suggest that the occurrence of the dissipation peak in the imaginary part of the complex susceptibility X" (to, T) is due to the skin effect known for electrical transport in metals in the normal state. At fixed field H, the peak temperature Tp(tn, H) increases with increasing frequency of the superimposed AC probing field, and does not coincide with the irreversibility temperature T* (H) < Tp for magnetization obtained in the static limit to-. 0. A phase diagram is presented which includes the DC irreversibility line H*(T), the peak positions Hp (to, T), the experimentally resolved zero-resistivity fields Hp=0(T), and the crossover fields from activated to diffuse resistive behavior, Hk(T), all measured on the same YBa2Cu307 single crystal.
Journal of Superconductivity and Novel Magnetism, 2012
The objective of the work is to establish the contribution of superconductive granules and grain boundaries (weak links) in magnetoresistance ρ value of YBa 2 Cu 3 O 7−δ granular high-temperature superconductor (HTS) at T < T c. The current-voltage characteristics (CVCs) E(j) H ext =const of YBa 2 Cu 3 O 6.95 ceramic samples were measured in H ext (0 ≤ H ext ≤≈ 500 Oe) magnetic fields. The CVCs E(j) H trap =const of the samples magnetized in H treat magnetic fields were measured at H ext = 0. Based on the CVCs, ρ(j) H ext =const , ρ(H ext) j =const and ρ(j) H treat =const dependences were reestablished. The comparative analysis of ρ(j) H ext =const and ρ(H ext) j =const dependences indicates the magnetic field redistribution between grain boundaries and superconductive granules influence on transport and galvanomagnetic properties of granular HTS. The superconductive grain magnetoresistance ρ g was established to be significantly lower than ρ J value of Josephson medium.
Applied Superconductivity, 1995
We present measurements of hysteresis in the magnetoresistance of sintered YBaCuO. In analogy with hysteresis in current density and in harmonic generation, this is attributed to trapping of flux within the grains. This feature is used to track the penetration of magnetic field inside the superconducting granular regions.
Europhysics Letters (EPL), 1998
We propose the existence of an electric-field induced nonlinear magnetization in a weakly coupled granular superconductor due to time-parity violation. As the field increases the induced magnetization passes from para-to dia-magnetic behavior. We discuss conditions under which this effect could be experimentally measured in high temperature superconductors.
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